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The collection includes a variety of cartographic materials, antiquarian book and map dealer records, correspondence, published articles, bibliographic materials, newspaper clippings, and publications. Highlights of the collection include historical materials and correspondence related to early explorers in North America. Cartographic materials included in the collection consist of map facsimiles, slides, and photostatic reproductions.

This collection consists of 40 signed documents, 7 autographed letters signed, and 6 letters signed, relating to the civil and military administration of the British possessions of East and West Florida. This is an important collection of manuscript material, apparently all unpublished, related to East and West Florida, which was part of the British Empire just prior to the American Revolution. Both were obtained from Spain at the Treaty of Paris in 1763. West Florida was captured by Governor Galvez of Louisiana in 1781, and East Florida reverted to Spain and was evacuated in 1784. Included in this collection are materials related to the following persons and topics: Major John Campbell, Lt. Col. Ralph Walsh, General Sir Frederick Haldimand, George Johnstone (Governor of West Florida), Patrick Tonyn (Governor of East Florida), Lt. Col. James Bruce, Peter Chester (Governor of West Florida), Lt. Col. M. G. Glasier, Pensacola, Florida, Lt. Gov. Monforte Brown, fortifications at Pensacola, Florida and Savannah, Georgia, troop movements from Pensacola and Mobile to the Mississippi River, St. Augustine, Florida, James Moore, Rangers, Lord George Germain (Secretary of State for the Colonies), Charlestown, South Carolina, military and naval intelligence, Lords of the Treasury, construction in Pensacola, French and rebel attacks, Johnstown, New York, and London. There are 42 items on West Florida and 11 items on East Florida.

Collection of 17th-19th century newspapers from London and Nottingham, England and Edinburgh, Scotland. Includes MSS 90-13, MSS 90-14, MSS 90-15 and MSS 90-16.

Collection consists mainly of photocopies of original manuscripts in Spanish from Archivos General de Indias, Sevilla, Spain. There are a few translations in Spanish and English in holograph, a few typed copies of the translations and transcription, plus some holograph notes and typed pages of the manuscript by Dr. Boyd. These, the microfilm rolls, and other items that are included in the gift by Dr. Boyd are packed in separate envelopes, boxes and other containers.

Materials included in the Floridiana collection include maps, correspondence, photographs, and publications (1730-1970) pertaining to the development of Florida, government ordinances, and government reports relating to Florida.

Microfilm of the fonds des colonies serie C13A, Volumes 1-53, covering French occupation of North America, 1694-1819. Filmed as part of the Louisiana Colonial Records Project in 1980, the C13A series covers reports, letters, maps, and other materials on the French settlement and colonization of Louisiana, West Florida, Pensacola, the upper Mississippi River Valley, the Illinois Territory, Canada and other areas of North America. The size of this research archives is beyond the scope of this Guide to describe, but there is considerable data on settlements, Indians, transportation, forts, shipwrecks, battles and war, Jesuit activity, troop movements, and more. Most materials are in French language.